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Metallurgy

The LEAP® Microscope is particularly well suited to materials and metals analysis for characterizing and understanding:

  • Grain boundary segregation
  • Precipitate size, composition and distribution
  • Nanocyrstallization in amorphous alloys
  • Precipitate vs. bulk composition

To view a larger image, click on the image caption. To read about an application in more detail, please click on the title above the thumbnail or click on the Read More link..

 
Precipitates in Nickel based superalloy

Atom map showing precipitates in Ni-based Alloy 718.
Atom map of precipitates in nickel based Alloy 718, showing γ, γ', and γ'' phases. Read More...
Multiphase Precipitation in NU Cu-150 Steel

Copper-rich parcipitates in high-strength low-carbon steel.
Atom map of multiphase precipitation in high-strength, low-carbon steel. Read More...
3D analysis of the nanoscale microstructure of a Ferritic superalloy

Leap analysis volume (100 nm x 100 nm x 400 nm) of a FeNiAlCr alloy.
Many heat-resistant ferritic steels have superior thermal-expansion and thermal conductivity properties compared to Ni-based alloys, but are somewhat limited, by their mechanical properties, in their applications above 600 degrees C. Read More...
Ordered Gamma Prime in Ni-Base Superalloy

A gamma prime-Ni3(Al,Cr) precipitate in a nickel-base superalloy. The precipitate is delineated from the matrix by an aluminum iso-surface. The Al atoms are in red while the Cr atoms are shown in blue; Ni atoms are omitted for clarity.

Nickel-base superalloys have long been prized for their high strength and corrosion resistance at elevated temperatures for use primarily in aviation jet engines. Ordered gamma prime-Ni3(Al,Cr) precipitates such as the one shown to the left are responsible for the high-temperature strength of nickel-base superalloys.

Read More...

Electrodeposited Ni-Mn Alloy

Grain boundry segregation in Ni-Mn alloy

Mn addition to electrodeposited Ni film, showing segregation to grain boundry and second phase particles.

Read More...
Heat-resistant ferritic steel

LEAP image of a heat-resistant ferritic steel that used coherent (Ni,Fe) Al precipitates in a ferritic matrix to achieve good high temperature mechanical properties

The properties of steels can be dramatically changed by the presence of small quantities of certain elements, especially in the boundaries between a material's crystalline grains, called grain boundaries. Scientists have found that changes in properties can be related to changes in structure and composition at the microscopic level. Thus, metallurgists were excited about the potential of atom probe to characterize the structure and composition of steels at the highest possible spatial resolution. Read More...

Carbon Segrecation in Steel

Carbon Segregation to dislocations in steel.
Observations of carbon segregation in low carbon steel. Read More...
Cu precipitation-hardened model steel

583 nano-scale Copper-rich precipitates in an Fe-1.7at.% Cu precipitation-hardened model steel. Green: Fe atoms, red: Cu atoms.
With hundreds of precipitates in a single reconstruction, resolved with sub-nanometer spatial resolution, a meaningful description of a nano-scale precipitate microstructure becomes possible with statistically significant distributions. Submitted by Dieter Isheim, David N. Seidman and Morris E. Fine of Northwestern University. Read More...
Impurity Distribution

Impurity Distribution in Copper
The atom probe microscope is particularly suited to metallurgical research. The LEAP microscope provides the speed and analysis volume to provide researchers with necessary information for nano-structure research in metals. Read More...
 Other Resources
Contact imago for additional application information including:
A list of customer publications
Review articles
Slides from an atom probe short course (IFES 2006)
Specimen preparation (Ultramicroscopy)
Atom by Atom 3D analysis of high-k films
Analysis software capabilities
Microscopy Today article
Microscopy and Analysis article
Solid State Technology article
Three dimensional mapping of dopants (Applied Physics Letters)
Nanomagnetic material characterization (Thin Solid Films)
Nanometallurgy
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Phone: (608) 274-6880
Fax: (608) 442-0622

 
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