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  Home >> Applications>> Semiconductors
 
Semiconductors

Traditionally atom probe was not a useful technique for non-conductive or semiconducting sample types. Imago's introduction of the laser pulser in 2005 enables many semiconducting samples to be measured with the LEAP 3000X Si. Key applications for semiconductor metrologists include the quantitative, 3d mapping of dopant distributions, compositional analysis of high-k films, quantitative measurement of clustering at interfaces, and silicides. In addition to these already established applications, new applications are emerging rapidy.

"Mapping dopants has been the industry Holy Grail for the past 30 years." - NSF Microscopy Panel

To view a larger image, click on the image caption. To read about an application in more detail, please click on the title above the thumbnail or click on the Read More link..

 
Lateral Dopant Distribution in a Transistor Structure

3D reconstruction of a patterned semiconductor test structure. Polysilicon deposited on a <100> single crystal silicon wafer. The As dopants are shown as purple spheres. 

As transistor structures continue to shrink to keep pace with Moore's Law the existing analysis and metrology techniques currently in use will no longer be sufficient to fully characterize the nanoscale devices. Atom probe has the unique capability to characterize the next-generation technology cycles by mapping the spatial distribution and chemical identity of dopants on the atomic scale.

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High-k

A thin hafnium dioxide high-k layer analyzed on a LEAP3000XSi.

In recent years the scaling of microelectronic devices to smaller and smaller dimensions to keep pace with Moores Law has been made possible by reducing the thickness of the silicon dioxide dielectric. The result has been a gate dielectric just a few atomic layers thick through which electrons can tunnel when the transistor is in the off state which increases power consumption and heat generation. This has spurred research into the use of high-k oxides to replace silicon dioxide in the gate insulator in order to improve performance with a thicker oxide. The atom probe has been used to characterize the morphology and composition of high-k films in three dimensions to aid in the development of these devices.

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Using Atom Probe Tomography (APT) to Characterize a SiGe Process

TEM cross-section of Intel PMOS courtesy of Chipworks

We detail the motivation and importance to the semiconductor industry of selective SiGe deposition. The challenges of this process are discussed especially process integration issues and pattern dependent deposition.

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B Implanted Through a Screen Oxide

3D mapping of B dopant (light blue) implanted through a screen oxide (light gray).
Cross-sectional view of a three-dimensional atom map of B dopant (light blue spheres) implanted through a screen oxide (gray spheres). A polysilicon layer was deposited on top. Read More...
Silicidation of NiPd/Si

Silicidation of NiPd/Si system with 5 at. % Pd in Ni. Uniform distribution of Pd in NiSi Segregation of Pd at NiSi/Si interface. Ni shown as green, Si blue, Pd red.
Metal silicide thin films are integral parts of all microelectronics devices. They have been used as ohmic contacts, Schottky barrier contacts, gate electrodes, local interconnects, and diffusion barriers. With advances in semiconductor device fabrication technology, the shrinkage in line width continues at a fast pace. The International Technology Roadmap for Semiconductors (ITRS) predicted that in 2005, in the 90 nm generation devices, the gate length and thickness of silicide at the contact window would be 32 nm and 20 nm, respectively. In the year 2007, for the 65 nm generation devices, these numbers are predicted to further decrease to 25 nm and 17 nm, respectively. Read More...
Boron dopants in SiGe

Boron in Si and SiGe (Si in grey, B in blue and Ge in green)
Layered films of SiGe, Boron doped Si and Boron doped SiGe. Read More...
Dopant Mapping

Boron Dopants in Silicon
Dopant mapping has long been considered the "holy grail" of the semiconductor industry. The Imago Atom Probe family of products makes accurate dopant mapping a reality for semiconductor metrologists. Read More...
 Other Resources
Contact imago for additional application information including:
A list of customer publications
Review articles
Slides from an atom probe short course (IFES 2006)
Specimen preparation (Ultramicroscopy)
Atom by Atom 3D analysis of high-k films
Analysis software capabilities
Microscopy Today article
Microscopy and Analysis article
Solid State Technology article
Three dimensional mapping of dopants (Applied Physics Letters)
Nanomagnetic material characterization (Thin Solid Films)
Nanometallurgy
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Phone: (608) 274-6880
Fax: (608) 442-0622

 
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